2-Trifluoromethyl-1H-benzimidazol-3-ium tetrafluoroborate–2-trifluoromethyl-1H-benzimidazole–water (1/1/1)

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2-Trifluoro­methyl-1H-benzimidazol-3-ium perchlorate

In the title salt, C(8)H(6)F(3)N(2) (+)·ClO(4) (-), the atoms of the benzimidazole ring (including H atoms) are nearly coplanar (r.m.s. deviation of the fitted atoms = 0.0122 Å) and the triflouromethyl group lies out of this plane. The perchlorate anion adopts a distorted tetra-hedral conformation with the Cl-O bond distances ranging from 1.412 (3) to 1.439 (2) Å. The benzimidazolium cations ar...

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2-Trifluoro­methyl-1H-benzimidazol-3-ium nitrate

Ihe title salt, C(8)H(6)F(3)N(2) (+)·NO(3) (-), the F atoms of the triflouromethyl group are disordered over two sets of sites in a 0.58 (2):0.42 (2) ratio. In the crystal, N-H⋯O hydrogen bonds link the cations and anions into chains running parallel to the b axis. There is π-π stacking between symmetry-related benzene rings with a centroid-centroid distance of 3.949 (3) Å. The crystal studied ...

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1H-Benzimidazol-3-ium-2-carboxyl­ate dihydrate

The title compound, C(8)H(6)N(2)O(2)·2H(2)O, crystallized as a zwitterion with the carboxyl group deprotonated and the imidazole group protonated. The dihedral angle between the benzimidazole ring and the pendant -CO(2) group is 0.62 (2)°. In the crystal, mol-ecules are linked into a three-dimensional network by N-H⋯O and O-H⋯O hydrogen bonds.

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2-(2-Hy­droxy-3-meth­oxy­phen­yl)-1H-benzimidazol-3-ium perchlorate

In the title mol-ecular salt, C(14)H(13)N(2)O(2) (+)·ClO(4) (-), the ring systems in the cation are almost coplanar [dihedral angle = 5.53 (13)°]. Intra-molecular N-H⋯O and O-H⋯O hydrogen bonds generate S(6) and S(5) rings, respectively. In the crystal, the two H atoms involved in the intra-molecular hydrogen bonds also participate in inter-molecular links to acceptor O atoms of the perchlorate...

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1-{2-[2-(1H-Benzimidazol-1-yl)eth­oxy]eth­yl}-1H-benzimidazol-3-ium hexa­fluoro­phosphate

In the title salt, C(18)H(19)N(4)O(+)·PF(6) (-), the dihedral angle between the benzimidazolium and benzimidazole ring systems is 16.24 (2)°. In the cation, a π-π inter-action is observed between the imidazolium ring and the benzene ring of the benzimidazole ring system [centroid-centroid distance = 3.5713 (11) Å]. The PF(6) (-) ion is disordered over two sites, with occupancies of 0.895 (2) an...

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online

سال: 2012

ISSN: 1600-5368

DOI: 10.1107/s1600536812010847